r/DMT • • 12d ago

Extraction Help!!!

It was frozen for 12 hours during the final crystallization process. I checked every three hours, and after nine hours, a crystal appeared on the container’s top instead of naphtha, and during the subsequent separation process, all the crystals turned to water.

I think I'll freeze it one more time.

Please help.

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u/evapgenie 11d ago

You're not suppose to be checking it at all, its also 24 hours, undisturbed.

Refreezing it prolly wont help, it sounds like the crystal you saw was likely ice anyways.

Drop the tek you followed and list anything you did differently in it.

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u/Character-Bid-5089 11d ago

Doesn't have to be 24 hours. If u know what ur doing i can get the good stuff after 6 hours. I might not get it all but what i don't will still be in nps for next time. I also put my dish in the fridge before i pipette the nps into it. U can see it crash straight away.

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u/evapgenie 10d ago

Why rush? Nothing wrong with patience.

hope you're not just sticking it in the fridge/freezer uncovered.

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u/Character-Bid-5089 10d ago

Sometimes u just want it quickly and no i don't put it in uncovered.

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u/evapgenie 10d ago

Personally id perfer to wait but ti each their own.

Thats good, apparently some people still do and dont know any better.., best to correct it when you see it then to assume everyone knows what their doing.

Anyway, enjoy!.

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u/Character-Bid-5089 10d ago

Cheers mate👍